Preparation of Long Afterglow PhotoluminescentMatedal SrAI2O4 ： Eu^2＋ , Dy^3 ＋ and ItsLuminescent Property

Long lasting strontium aluminate phosphors were synthesized by means of coated precipitation in the experiment. SrA12O4 monoclinic phase with long afterglow was synthesized at 1 100 ℃ with the aid of H3BO3,and the synthetic temperature decreased about 100 ℃-150 ℃ than in solid state reaction. The process of heat treatment was studied by TG-DTA. The phase compositions of powders were analyzed by XRD. The micrographs of the samples were investigated by SEM and the luminescent properties were researched by optical spectrum. The effects of H3 BO3 on the phase composition and microstructure of the calcined powders were investigated. The results indicated that H3BO3 accelerated the formation of SrAl2O4 by consuming the intermediate phase. The addition of Dy2O3 stimulated the afterglow property due to the increase in the depth of the trap center in the materials.     

Modeling of tool-chip contact length for orthogonal cutting of Ti-6Al-4V alloy considering segmented chip formation

In this work, the orthogonal cutting experiments on Ti-6Al-4V alloy were conducted at different cutting speeds(10—160 m/min)and feed rates(20—160 μm/rev). The tool-chip contact length was measured by the track of tool rake face; meanwhile, the chip morphology caused by the localized and overall chip deformation was characterized by the degree of segmentation and the chip compression ratio, respectively. These parameters were analyzed and calculated according to the segmented chip morphology. In addition, three modified models considering the overall chip deformation and the localized deformation of adiabatic shear band were proposed, and the constants of the models were calculated by the genetic algorithm optimization. Considering the overall and localized chip deformation, the value and variation trend of the tool-contact length predicted by these three models agreed well with the experimental results.     

A Family of Exact Solutions fort the Nonlinear Schrodinger Equation

In this paper,the nonlinear Schrodinger(NLS)equation was analytically solved.Firstly,the stationary solutions of NLS equation were explicitly given by the elliptic functions.Then a family of exact solutions of NLS equation were botained from these stationary solutions by a method for finding new exact solutions from the stationary solutions of integrable evolution equations.     

Test on evaluation method for biodegradability of lubricants

Using carbon tetrachloride （CCl4） as extraction agent, the activated sludge from Tianjin Jizhuangzi Sewage Treatment Plant as inoculum, the test study on biodegradability of lubricants was carried out. The test flasks containing the mineral medium, the test oil and the inoculum were placed in incubation together with flasks containing poisoned blanks for periods of 0 and 21 days, respectively. Flasks containing the reference materials in place of the test oil were run in parallel. At the end of the incubation period, the contents of the flasks were subjected to sonic vibration, and were acidified and extracted by using CCI4. The extracts were then analysed by infra-red （IR） spectrometer to measure the maximum absorption of the C-H stretch of CH2-CH3 band at wavelength of 2 930 cm^-1. The absorption values were used to calculate the residual oil contents of the poisoned and test flasks. Consequently the biodegradability of the test oil was calculated. The test results indicate that the differences in the biodegradability of test materials in different tests are within 5.5%, and consistent with the data described in Coordinating European Council （CEC） L-33- A-93. The biodegradability of lubricants can be evaluated by this method effectively.     

In的掺杂对化学水浴沉积SnS薄膜电阻率的影响

SnS and SnS：In films were deposited onto glass substrates by chemical bath technique. The structure and surface morphology of the SnS：In films were studied by X-ray diffraction （XRD） and scanning electron microscope （SEM） respectively. Energy dispersive spectroscopy （EDS） showed the existence of In in the films. The undoped SnS film exhibited a rather high resistivity and InCl3 could reduce the resistivity of these films by two orders approximately. The band gaps of the SnS and SnS：In films were evaluated from the optical transmission spectra.     

关于离散复杂动力学网络同步现象的稳定性分析

In this paper,by using both the linear stability analysis and Lyapunov function approach,some conditions for stabilizing synchronization behavior in a discrete-time complex dynamical network were derived.These conditions were determined by the coupling strength and the eigenvalues of coupling configuration matrix.Furthermore,some explicit results were obtained when the coupling map between the nodes is equal to the dynamics function of the network,which implies that the product of the coupling strength and the eigenvalues is bounded.     

Characteristics of bifurcation and buckling load of space truss in consideration of initial imperfection and load mode

This study investigated characteristics of bifurcation and critical buckling load by shape imperfection of space truss,which were sensitive to initial conditions.The critical point and buckling load were computed by the analysis of the eigenvalues and determinants of the tangential stiffness matrix.The two-free-nodes example and star dome were selected for the case study in order to examine the nodal buckling and global buckling by the sensitivity to the eigen buckling mode and the analyses of the influence,and characteristics of the parameters as defined by the load ratio of the center node and surrounding node,as well as rise-span ratio were performed.The sensitivity to the imperfection of the initial shape of the two-free-nodes example,which occurs due to snapping at the critical point,resulted in bifurcation before the limit point due to the buckling mode,and the buckling load was reduced by the increase in the amount of imperfection.The two sensitive buckling patterns of the numerical model are established by investigating the displaced position of the free nodes,and the asymmetric eigenmode greatly influenced the behavior of the imperfection shape whether it was at limit point or bifurcation.Furthermore,the sensitive mode of the two-free-nodes example was similar to the in-extensional basis mechanism of a simplified model.The star dome,which was used to examine the influence among several nodes,indicated that the influence of nodal buckling was greater than that of global buckling as the rise-span ratio was higher.Besides,global buckling is occurred with reaching bifurcation point as the value of load ratio was higher,and the buckling load level was about 50%-70% of load level at limit point.     

确定轴向运动梁固有频率的多尺度法

The natural frequencies of an axially moving beam were determined by using the method of multiple scales. The method of second-order multiple scales could be directly applied to the governing equation if the axial motion of the beam is assumed to be small. It can be concluded that the natural frequencies affected by the axial motion are proportional to the square of the velocity of the axially moving beam. The results obtained by the perturbation method were compared with those given with a numerical method and the comparison shows the correctness of the multiple-scale method if the velocity is rather small.     

Metal Chlorides Supported Solid Catalysts for F-C Acylations of Arenes

A series of metal chlorides supported solid catalysts were prepared by simple wet impregnation method. Their catalytic performances for Friedel-Crafts acylation of toluene with benzoyl chloride were evaluated and the excellent results were obtained over Fe Cl3/Si O2. These catalysts were characterized by BET, NH3-TPD and FT-IR of pyridine adsorption to clarify the structure-activity relationship. It was found that Fe Cl3/Si O2 has larger pore size and pore volume than other catalysts, which increased the accessibility of the catalyst. In addition, Fe Cl3/Si O2 exhibited higher molar ratio of Lewis acid sites and Brφnsted acid sites, which might be another reason for the increase of toluene conversion. Furthermore, the reaction parameters, including temperature, time and molar ratio, were optimized. Under the optimized conditions, 91.2%, conversion and 82.0%, selectivity were obtained. Meanwhile, the generality of the catalyst was demonstrated by the acylations of alkyl substituted aromatics. Finally, the catalyst was reused for four runs with slight loss in catalytic activity, which attributed to the drain of the active component.     

Measurement of moment of inertia based on hilbert transform

A measurement model based on torsion pendulum was established,in which nonlinear damping and nonlinear restoring force were considered.The calculation method of the moment of inertia was based on Hilbert transform.The motion of torsion pendulum showed the time-frequency characteristics due to the nonlinear factors,which were validated by the experimental data.The analytical signal was formed by Hilbert transform of the angular displacement signal of the test object.The moment of inertia can be computed by the instantaneous undamped natural frequency with Hilbert transform.Prior to the implementation of Hilbert transform,the empirical mode decomposition was used to filter the experimental signal.The moment of inertia of the test object was measured by the torsion pendulum system.The experimental results show that the relative measurement error of the moment of inertia was within 0.7%,which indicated the validity of the measurement method.     

泰国南邦省陶瓷厂细颗粒物对大鼠肺部的影响(英文)简

Background： Lung cancer ranks as the fifth largest of all cancer cases in Thailand. However, it is the first leading cancer in the northern part of Thailand （data from 2003-2007）. There are several predisposing causes that lead to lung cancer and one important inducement is particulate matters （PMs）. Lampang Province in Thailand is famous for the ceramic industry, where there are over 200 ceramic industrial factories. PMs are produced during the ceramic manufacturing process and spread throughout all of the working areas. It is very possible that workers could directly inhale PM-contaminated air during working hours. Objective： This study focuses on the toxic effects of PMs collected from ceramic factories on genes and lungs of rats. Methods： PMs collected from six ceramic factories in Lampang Province were extracted using dimethyl sulfoxide （DMSO）. The inductively coupled plasma mass spec- trometry （ICP-MS） and inductively coupled plasma optical emission spectrometry （ICP-OES） were used to analyze the chemical elements at lower and higher concentrations, respectively. Then, the toxicity of PMs on the genes was ex- amined by the Ames test, and subsequently, the effect of PMs on DNA was examined by quantifying the amount of 8-hydroxy-2＇-deoxyguanosine （8-OHdG）. Finally, the toxicity of the PMs on rat＇s lungs was examined by histology. Results： As chemical elements of lower concentrations, cadmium, chromium, nickel, copper, and lead were detected by ICP-MS. As chemical elements of higher concentrations, manganese, magnesium, zinc, iron, potassium, calcium, and sodium were detected by ICP-OES. No mutagenicity in Salmone/la typhimurium was found in the PM extracts from all six factories by utilizing the Ames test. In the histological study, the reduction in spaces of alveolar ducts and sacs, and terminal bronchioles, the thickening of interstitial connective tissues were noted by PM extracts in high amounts （100 and 350 pg）. Female rats were more sensitive to PM extracts than males in terms of their pulmonary damages. Conclusions： PMs were not mutagenic to S. typhimurium but can damage the lung tissue of rats.     

校园中的流浪者[二]

Then there were the freight trains, the motive power of which was mules and oxen. It was necessary to carry forward supplies and bring back the crude products of the country. The Chihuahua wagon was drawn sometimes by twelve, sometimes by twenty mules, four abreast in the swing,the leaders and wheelers being single teams. For mutual protection trains were made up of from ten to twentywagons.     

Roots of pioneer trees in the lower sub-tropical area of Dinghushan, Guangdong, China

Representative pioneer tree root systems in the subtropical area of South China were examined with regard to their structure, underground stratification and biomass distribution. Excavation of skeleton roots and observation of fine roots of seven species including the Euphorbiaceae, Theaceae, Melastomataceae, Lauraceae and Fagaceae families was carried out. The results showed that： （1） Pioneer tree roots in the first stage of natural succession were of two types, one characterized by taproot system with bulky plagiotropic branches; the other characterized by flat root system with several tabular roots. The late mesophilous tree roots were characterized by one obvious taproot and tactic braches roots up and down. Shrub species roots were characterized by heart fibrous root type featured both by horizontally and transversally growing branches. Root shapes varied in different dominant species at different stages of succession. （2） Roots of the different species varied in the external features-color, periderm and structure of freshly cut slash. （3） In a set of successional stages the biomass of tree roots increased linearly with the age of growth. During monsoon, the total root biomass amounted to 115.70 t/ha in the evergreen broadqeaved forest; 50.61 t/ha in needle and broad-leaved mixed forest dominated by coniferous forest; and 64.20 t/ha in broad-and needle-leaved mixed forest dominated by broad-leaved heliophytes, and are comparable to the underground biomass observed in similar tropical forests. This is the first report about roots characteristics of forest in the lower sub-tropical area of Dinghushan, Guangdong, China.     

Simulated moving bed separation of tocopherol homologues: simulation and experiments

Chromatograms of tocopherol homologues were obtained by a column of analytical size （inner diameter （ID） 0.46 cm cm×10 cm） packed with silica gel. Adsorption isotherms and film mass-transfer coefficient were estimated from the chromatograms by using a general rate model, which considers axial dispersion, external mass-transfer and intraparticle diffusion. Based on the obtained isotherms and mass-transfer coefficient, the separation process of tocopherol homologues on simulated moving bed （SMB） was simulated using the same model. According to the simulated results, a mixture of α-, γ-, δ-tocopherols and other impurities was separated on an SMB equipment. The SMB equipment was composed of 8 columns of ID 2 cm× 1 0 cm, with 2 columns in each section. The solid phase was silica gel, and the mobile phase was n-hexane/2-propanol （99/1 by volume）. γ- and δ-tocopherols of purity greater than 98% were obtained with recovery greater than 98%. The effects of operating conditions （flow rates and switching time） on the performance of SMB were studied by both simulation and experiments. It was found that all the simulation results were quite close to the experimental results. We conclude that process development and optimization of operating conditions of SMB by simulation are feasible.     

Effect of selected fungi on the reduction of gossypol levels and nutritional value during solid substrate fermentation of cottonseed meal

The objective of this work was to investigate the effect of six individual strains of fungi on the reduction of gossypol levels and nutritional value during solid substrate fen＇aentation of cottonseed meal （CSM）. Six groups of disinfected CSM substrate were incubated for 48 h after inoculation with either of the fungi C. capsuligena ZD- 1, C. tropicalis ZD-3, S. cerevisae ZD-5, A. terricola ZD-6, A. oryzae ZD-7, or A. niger ZD-8. One not inoculated group （substrate） was used as a control. Levels of initial and final free gossypol （FG）, crude protein （CP）, amino acids （AA） and in vitro digestibility were assayed. The experiment was done in triplicate. The experimental results indicated that microbial fermentation could greatly decrease （P〈0.05） FG levels in CSM. The detoxification efficiency differed between the species of microorganisms applied. From the perspective of reducing CSM potential toxicity, C. tropicalis ZD-3 was most successful followed by S. cerevisae ZD-5 and A. niger ZD-8. They could reduce FG levels of CSM to 29.8, 63.07 and 81.50 mg/kg based on DM （dry matter）, respectively, and their detoxification rates were 94.57%, 88.51% and 85.16%, respectively. If crude protein, amino acids content and their in vitro digestibility were also taken into account, Aniger ZD-8 may be the best choice. The CP content of CSM substrate fermented by C. tropicalis ZD-3 and A. niger ZD-8 were improved by 10.76% and 22.24%; the TAA （total amino acids） contents were increased by 7.06% and 11.46%, and the EAA （essential amino acids） were raised by 7.77% and 12.64%, respectively. Especially, the levels of methionine, lysine and threonine were improved greatly （P〈0.05）. The in vitro CP digestibility of CSM fermented by C. tropicalis ZD-3 and A. niger ZD-8 was improved by 13.42% and 18.22%, the TAA were increased by 17.75% and 22.88%, and the EAA by 16.61% and 21.01%, respectively. In addition, the in vitro digestibility of methionine, lysine and threonine was also improved greatly （P〈0.05）.     

Mn3+～甲苯非均相体系的氧化反应动力学

The reaction kinetics of the heterogeneous oxidation oftoluene with Mn^3 was studied by considering the effects of disproportionation of Mn^3 in reaction system,a “parallel”modulus was set up.And then the concentration of Mn^3 in disproportionation and the concentration of benzaldehyde in oxidation were respectively determined in turn.the rate constant,order and pseudo-activation energy of the heterogeneous oxidation were obtained by mathematical deduction and the kinetic equation was concluded.In addition,the reaction mechanism was analyzed.It shows that the results are completely consistent with modulus.     

Genetic analysis for brix weight per stool and its component traits in sugarcane (Saccharum officinarum)

Brix weight per stool (BW) of sugarcane is a complex trait, which is the final product of a combination of many components. Diallel cross experiments were conducted during a period of two years for BW and its five component traits, in- cluding stalk diameter (SD), stalk length (SL), stalk number (SN), stalk weight (SW), and brix scale (BS) of sugarcane. Phenotypic data of all the six traits were analyzed by mixed linear model and their phenotype variances were portioned into additive (A), dominance (D), additive×environment interaction (AE) and dominance×environment interaction (DE) effects, and the correlations of A, D, AE and DE effects between BW and its components were estimated. Conditional analysis was employed to investigate the contribution of the components traits to the variances of A, D, AE and DE effects of BW. It was observed that the heritabilities of BW were significantly attributed to A, D and DE by 23.9%, 30.9% and 28.5%, respectively. The variance of A effect for BW was significantly affected by SL, SN and BS by 25.3%, 93.7% and 17.4%, respectively. The variances of D and DE effects for BW were also significantly influenced by all the five components by 5.1%～85.5%. These determinants might be helpful in sugarcane breeding and provide valuable information for multiple-trait improvement of BW.     

KdV方程的新Wronskian解

The novel Wronskian solutions of the KdV equation were obtained as limits of the soliton solutions in the Wronskian form. These solutions were verified by direct substitution to satisfy the bilinear derivative form of the KdV equadon and its Backlund transformation.     

Using fracture grouting to lift structures in clayey sand

An inclined seven-story reinforced concrete building was leveled by a fracture grouting technique with quick-setting grout on a differential thickness of a clayey sand layer. The permeability and strength of clayey sand were controlled by clay content, although sand was the primary component of the foundation soil. The elevations of the building columns at basement level were closely monitored to record both the heaved volume of mat foundation after grouting and the settled volume during pore pressure dissipation. During the stabilizing stage of grouting, the foundation soil was densified by the repetitive fracturing process, which resulted in the lateral movement of the foundation soil. When the grout is less able to push soil laterally than upwards, the building starts to lift, the so-called lifting stage of grouting. The grouting efficiency is influenced by soil type, soil stress history, and foundation pressure. A final grouting efficiency of 27% and a linear relationship between grout use and percentage of elevation were obtained when this building was successfully and permanently leveled.     

Bayesian mapping of neural tube defects prevalence in Heshun County, Shanxi Province, China during 1998-2001

Objective： To estimate the prevalence rates of neural tube defects （NTDs） in Heshun County, Shanxi Province, China by Bayesian smoothing technique. Methods： A total of 80 infants in the study area who were diagnosed with NTDs were analyzed. Two mapping techniques were then used. Firstly, the GIS software ArcGIS was used to map the crude prevalence rates. Secondly, the data were smoothed by the method of empirical Bayes estimation. Results： The classical statistical approach produced an extremely dishomogeneous map, while the Bayesian map was much smoother and more interpretable. The maps produced by the Bayesian technique indicate the tendency of villages in the southeastern region to produce higher prevalence or risk values. Conclusions： The Bayesian smoothing technique addresses the issue of heterogeneity in the population at risk and it is therefore recommended for use in explorative mapping of birth defects. This approach provides procedures to identify spatial health risk levels and assists in generating hypothesis that will be investigated in further detail.