过冷液相区内轧制温度对Zr52.5Al10Ni10Cu15Be12.5大块金属玻璃表面形貌的影响

Surface morphologies of Zr52.5 Al10 Ni10 Cu15 Be12.5 bulk metallic glass after being rolled at both a temperature around T9 and near （ Tx - 50） K were investigated with a scanning electron microscopy. Macroscopic and microscopic observation results show that squamae, cracks, steps and wedges exist on the surface when the samples were rolled at temperatures around Ty. However, a smooth and fiat surface appears when the samples were rolled at temperatures near （ Tx - 50） K. These results indicate that the mode of deformation in the supercooled liquid region is a partially homogeneous flow at a temperature around T9, and a fully homogeneous one at temperatures near （ Tx - 50） K. According to the results, it is more feasible to roll the amorphous alloys at temperatures near （ Tx - 50） K to obtain parts with smooth and fiat surface.     

压力对Zr41.2Ti13.8Cu12.5Ni10Be22.5块体非晶合金晶化行为的影响

介绍了用于压力测量的新型bridgman装置，并结合X射线衍射分析技术（XRD）研究了常压、高压条件下Zr41．2Ti13．8Cu12．5Ni10Be22．5块体非晶合金的晶化。结果表明，在相同的退火条件下（400℃，退火3小时），增大压力有利于Zr41．2Ti13．8Cu12．5Ni10Be22．5块体非晶合金的晶化；压力越大获得晶化相的晶粒尺寸越大。     

Zr_(52．5)Al_(10)Ni_(10)Cu_(15)Be_(12．5)大块金属玻璃的高温宏观硬度

The hot hardness behavior of Zr_(52.5)Al_(10)Ni_(10)Cu_(15)Be_(12.5) bulk metallic glass is studied from ambient temperature to the temperature over T_x (the onset crystallization temperature) using a hot macro-hardness tester and scanning electron microscopy (SEM).The results show that the hot hardness behavior of Zr_(52.5)Al_(10)Ni_(10)Cu_(15)Be_(12.5) bulk metallic glass can be classified into 4 zones:the glassy zone in which the hardness almost linearly decreases with the increase of temperature,the viscoelastic zone in which the hardness is nearly unchanged,the viscous flow zone in which the hardness quickly tends towards near zero with temperature,and the crystallization zone in which the hardness sharply increases.The high temperature deformation behavior and the easy processable deformation region for bulk metallic glasses are also discussed on the basis of the hot marco-hardness.     

Cu-Zr基金属玻璃的形成能力及力学性能研究

用铜模吸注方法制备了不同直径的Cu47.5Zr47.5Nb5金属玻璃,并用X-Ray对制备的金属玻璃进行了结构测定,同时对金属玻璃进行了压缩实验及断口分析。实验结果表明,Cu-Zr基金属玻璃的形成能力受到Nb的加入和吸铸直径的影响:相对于直径为2mm的金属玻璃,直径为3mm及5mm的金属玻璃的塑性和压缩强度都有明显的降低,其综合性能明显下降,表明直径对合金性能的影响相当大。     

高应变率下Zr基非晶合金的单轴压缩断裂行为

采用分离式Hopkinson压杆装置(SHPB)和扫描电镜(SEM)技术研究了不同高应变率下Zr基非晶合金样品(Zr55Cu30Al10Ni5)的变形行为和断口形貌。研究发现与准静态压缩形变相比,高应变率水平(3400 s-1和1900 s-1)下,非晶合金样品断裂应力显著降低,最大降低约达40%。扫描电镜形貌观察表明,非晶合金的高速断裂发生在一条主剪切带上,主剪切面偏离45°最大切应力面。同时断口形貌为明显的脉络花样,并覆盖有大量液滴状和不规则形状熔融物,表明高应变率下断裂表面温升较准晶态断裂有所增加。     

Influence of Rolling Temperature in Supercooled Liquid Region on the Surface Morphology of Zr_(52.5)Al_(10)Ni_(10)Cu_(15)Be_(12.5) Bulk Metallic Glass

1IntroductionSince a non-noble bulk metallic glassy alloy was dis-covered byInoue ,et al.[1]in 1988 , many stable amor-phous alloy systems with higher glass-forming abilityand lower critical cooling rates have been developed .Among them, Zr-based metallic glassy alloys are in-tenselyinvestigated because of their wider supercooledliquid region and other favorable thermodynamic andmechanical properties .In general ,surface morphologyof amorphous alloy parts is veryi mportant forindustri-al and …