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1.
ABSTRACT

A controversial set of elite jewels assumed to be of early medieval period, recovered in 1937–1938 from a burial site in Matzhausen (northeastern Bavaria) was investigated to determine their technological coherency as well as their authenticity. The discovery of these jewels was exploited by German nationalists to argue that the material culture observed in Bohemia and Moravia in the ninth century had Germanic roots. The circumstances of their discovery, however, remain unclear. Research in archives demonstrated the involvement of the SS Ahnenerbe organisation in the recovery of the jewels. Are these jewels authentic or are they forgeries manufactured or modified by a modern craftsman to serve German expansionist nationalism? Three jewels recovered in the grave – a gombik (hollow spherical pendant), an earring with chainlet, and a zoomorphic figurine – were investigated using scanning electron microscopy (SEM) coupled with energy-dispersive X-ray spectroscopy (EDX), X-radiography, and stereomicroscopy. The investigation revealed a very heterogeneous set of objects with respect to technology and state of preservation. It also uncovered repairs and past invasive interventions involving modern metal and solder. Comparison with similar types of jewels from Bohemia and Moravia points to important differences in construction and technology, which confirms the uniqueness of this set of objects and casts suspicion on their authenticity.  相似文献   

2.
《文物保护研究》2012,57(1):59-64
ABSTRACT

We analyzed 53 historical textile samples from a collection of caftans and brocades dating between the sixteenth and nineteenth century in the Topkapi Palace Museum (TPM) by scanning electron microscopy with energy dispersive X-ray spectroscopy (SEM-EDX). Data were collected on the type, dimensions, elemental composition, and level of corrosion. The technique is presented in this work as an efficient and micro-destructive tool for the characterization of the structure of historical metal threads. SEM-EDX analysis for different energies was performed on a selection of gold and silver threads belonging to the historical textiles. The results were interpreted via laboratory prepared samples of gilt Ag and sulfur reacted Ag at different thicknesses for Au and Ag2S layers respectively. A series of Au–Ag alloys for different Au/Ag ratios were prepared for comparative analysis. The threads were made of metal strips wound around a silk core. Metal wires and flat strips were also used. The use of differential energies allowed for differentiating strips and wires made of homogeneous silver and gold alloys from the ones coated with a thin gold layer. Analysis of EDX data revealed that the Au film thickness was very thin (10–60?nm). Formation of Ag2S layers over the thin Au film as thick as 1.5?µm was taking place. Formation of thinner Ag2S layers over non-gilt Ag suggested different reaction mechanisms for gilt and non-gilt cases.  相似文献   

3.
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