304L不锈钢粉末的温压行为与烧结行为

比较了304L不锈钢粉末在不同压力下温压成形与冷压成形的生坯密度和生坯强度,并研究了烧结温度对304L粉末烧结性能的影响。试验结果表明,304L不锈钢粉末的温压生坯密度和生坯强度都高于冷压生坯密度和强度。在800 MPa的压制压力下,304L的温压生坯密度为7.07 g.cm-3,比冷压提高了0.24 g.cm-3,生坯强度为35.6 MPa,比冷压提高了22.8%。在1 300℃温度下真空烧结后,304L不锈钢粉末压坯的密度为7.50 g.cm-3,抗拉强度为471 MPa,延伸率为47.7%,硬度为65 HRB。     

烧结气氛对不锈钢粉末烧结性能的影响

研究了真空和分解氨气氛对316L和304L不锈钢粉末烧结性能的影响。结果表明:1300℃时,真空烧结的密度比分解氨气氛烧结的高;由于氮的渗入,分解氨气氛烧结的抗拉强度比真空烧结时高出很多,但延伸率却低了很多。     

烧结316L不锈钢粉末多孔材料压缩性能的研究

以316L不锈钢粉末为原料,采用模压成形与烧结工艺,制备出孔隙度为20%~45%的烧结316L不锈钢粉末多孔材料,分别采用1 150℃和1 200℃烧结温度.烧结316L不锈钢粉末多孔材料的压缩应力-应变曲线上第二区域和第三区域分界不明显.相同烧结温度下,烧结316L不锈钢粉末多孔材料的压缩屈服强度、压缩弹性模量随孔隙度的升高呈指数下降趋势.     

烧结316L不锈钢粉末多孔材料的K_(IC)性能研究

以316L不锈钢粉末为原料,采用模压成形与烧结工艺,制备出孔隙度为20%～45%的烧结316L不锈钢粉末多孔材料,分别采用了1 150℃和1 200℃烧结温度.研究了烧结温度、孔隙度对烧结316L不锈钢粉末多孔材料的断裂韧度的影响.结果表明:断裂韧度随孔隙度的升高呈下降趋势,但断裂韧度与孔隙度是一种非单调的函数关系.表面裂纹总是沿着烧结颗粒边缘、孔隙等结构薄弱环节扩展.     

氢化-脱氢钛压坯烧结实验研究

以氢化-脱氢(HDH)钛粉为原料,采用不同压坯压力和烧结温度,对常规烧结和微波烧结做了对比研究,实验表明:压坯压力在170MPa以上可获得较好烧结性能,微波烧结相对常规烧结可获得均匀的烧结组织,较好的烧结致密度和抗压强度.     

流动温压技术成形螺纹孔

研究了流动温压工艺的成形温度对W-34Ni-5Fe混合粉末横向压力的影响及横向压力和生坯密度在横向距离上的分布,并进行了带螺纹孔的十字形零件的成形实验。实验结果表明,流动温压成形时,混合粉末在横向距离上存在较大的压力分布,流动温压工艺在十字形零件的纵向和横向都能成形出完好的内螺纹。     

Ti(C,N)基超细金属陶瓷的制备及表征综合实验设计

设计了Ti(C,N)基超细金属陶瓷制备及表征综合实验。以Ti(C,N)-Mo2C-WC-Ni/Co系为研究对象,改变化学成分、湿磨工艺、生坯密度、烧结工艺,并研究上述因素对超细金属陶瓷微观组织和孔隙度、密度、硬度和强度等性能的影响。研究结果表明:WC和Mo2C的添加都会导致环形相的形成,微观形貌随添加量变化;球料比、研磨时间和球磨机转速对研磨效率的影响是一致的,但这些参数的过度增大会引起杂质的产生和设备的磨损;高的生坯密度有利于减小烧结后的孔隙度;烧结温度和时间对金属陶瓷的致密化和晶粒长大都有重要的影响。     

含氮节镍型QN2109Mo奥氏体不锈钢组织和性能

选择含氮节镍型QN2109Mo奥氏体不锈钢作为研究对象,采用XRD、TEM、SEM、EDS、摩擦磨损试验机和电化学工作站等检测手段,研究QN2109Mo不锈钢的组织结构、摩擦磨损性能以及耐腐蚀性能,并与316L不锈钢进行对比。实验结果表明:N原子主要以间隙固溶形式存在于QN2109Mo不锈钢中,对QN2109Mo不锈钢组织起到了细化作用,提高了QN2109Mo 不锈钢的硬度。在干摩擦状态下,QN2109Mo不锈钢的耐磨损性能优于316L不锈钢,其磨损机理为氧化磨损和磨粒磨损共同作用。在w(NaCl)为3.5%的溶液中,QN2109Mo不锈钢表现出比316L不锈钢更低的自腐蚀电流密度和更高的点蚀电位,具有更优异的耐NaCl 溶液腐蚀性能。     

316L不锈钢镀银板的真空热处理工艺

本文分别通过探讨真空环境下热处理温度和热处理时间对316L不锈钢镀银板性能的影响,从而确定316L不锈钢镀银板的最佳真空热处理工艺。     

预烧温度对电解锰渣坯块烧结性能的影响

锰渣中含有大量有害物质而污染环境,大量堆放或填埋是当前处理锰渣的主要方式。以黄土为对比实验,通过对锰渣在500~700℃间预烧,研究预烧后的锰渣在1040~1100℃烧结温度下的烧结特性。结果表明,随预烧温度和烧结温度的升高,锰渣坯块的烧失率增加,吸水率、气孔率急剧减小,而体积密度和抗折强度增大,这与超过1080℃时熔融液相的出现有关。经650~700℃预烧后的样品在1060~1080℃温度下烧结具有最佳的综合性能,其密度可达1.77~1.85 g/cm~3,抗折强度可达24.8~33.3 MPa,完全可用来制作建筑材料领域中的轻质烧结砖,或者作为相关建筑材料的辅助原料。     

Investigation of compaction and sintering behavior of SiC powder after ultra-fine treatment

Silicon carbide ceramics were prepared with SiC powder treated by the fluidized bed opposed jet mill as rawmaterials, and the effects of the ultra-fine treatment mechanism on the compaction and sintering behavior of SiC ceramicswere investigated. The results showed that the compacts had higher density and microstructure homogeneity when thesintering temperature of the compact was decreased; and that the surface microstructure, densification and mechanicalproperties of the sintered body could be ameliorated obviously.     

Investigation of compaction and sintering behavior of SiC powder after ultra-fine treatment

INTRODUCTION In powder compaction, the characteristics ofthe powder affect the compaction behavior and thequality of the pressed green body and its relativedensity, porosity, pore size distribution, sinteringand the consequent microstructure of the final sin-tered body. Superfine powder is prerequisite forpreparing high performance ceramic materials (Liu,1996; Lange et al., 1983; Lange, 1989). At present,most of the chemosynthesis methods are not suit-able for preparing industrial …     

粉末冶金温压成形新技术及其应用

介绍粉末冶金温压成形新技术的发展概况及其应用情况.在不久的将来,高性能铁基粉末冶金零件在汽车、机械工业中的应用将不断扩大,温压粉末冶金零件的潜在市场十分广阔.在此基础上指出在国内开展温压成形技术的研究具有重要现实意义.     

Effects of agarose concentration and addition on the properties of gel-cast 3Y-ZrO2 green and sintered bodies

Using agarose as a gel agent to prepare ceramics is a suitable non-toxic gel-casting method. The effects of agarose concentration and addition amount on gel-cast 3Y-ZrO_2 green and sintered bodies were investigated. Green bodies were prepared by gel-casting using an agarose solution of a different agarose mass fraction including 3.0%, 3.5%, 4.0%, 4.5%, 5.0% and 5.5%with an added amount of agarose in the green body at a mass fraction of 0.7%, and using the agarose solution of a mass fraction of4.5% with a different amount of added agarose including 0.6%, 0.7%, 0.8%, 0.9%, and 1.0% in terms of mass fraction. The green bodies were sintered at 1 600 °C for 4 h. The relative density, linear shrinkage, and bending strength of the green bodies, and the density, microstructure, bending strength, and fracture toughness of sintered samples were characterized and analyzed. Results show that comprehensive properties of green bodies made with 4.5%(in terms of mass fraction) agarose solution added to an mass fraction of agarose in the slurry at 0.6% were the best, of which the bending strength was 3.14 MPa, the linear shrinkage was below 4.3%, and the relative density is 57.3%. For sintered bodies, the best fracture toughness was 5.63 MPa m~(1/2), and the optimal density was 5.88 g cm~(-3).     

粉煤灰及矿粉对水泥基注浆料性能的影响

以硅酸盐和硫铝酸盐复合水泥为基材制作水泥基注浆材料,分别讨论了不同类型、不同掺量的粉煤灰和矿粉对水泥基注浆材料的流动度、容重、膨胀率、抗压抗折强度的影响。结果表明:粉煤灰能有效地增加水泥基注浆料的流动度,当粉煤灰掺量低于20%时,可以提高注浆料的塑性膨胀率,当Ⅰ级粉煤灰掺量为20%或Ⅱ级粉煤灰掺量为15%时,3 h膨胀率最高达1%;粉煤灰对注浆料的早期强度不利,但可以增强其后期强度。矿粉可以改善其流动度,随着矿粉的增加,注浆料的容重和膨胀率均呈下降趋势;矿粉对注浆料的28 d强度无显著影响,其早期强度随着矿粉的增加而下降,当S75矿粉掺量高于7%或S95矿粉掺量高于11%时,抗压抗折强度不满足规范要求。     

An experimental investigation of properties of polyethylene reinforced with Al powders

Mechanical and physical properties, such as tensile strength, elongation at break, modulus of elasticity, Shore D hardness, melt flow rate (MFR), and electrical and thermal conductivities of composites with high density polyethylene matrix reinforced with Al powders were investigated experimentally. Measurements of the mechanical and physical properties were performed up to a reinforcing component concentration of 30% volume Al powder and compared with mathematical models from the literature. The obtained results have shown that experimental data were in good agreement with theoretical data. The ultimate tensile strength (UTS) and elongation at break decreased with increasing Al powder content, which was attributed to the introduction of discontinuities in the polymer structure, and modulus of elasticity increased with increasing Al content. The composite preparation conditions allowed the formation of a random distribution of metallic particles in the polymer matrix volume for system high density polyethylene-Al (HDPE-Al). There was a cluster formation of Al particles at higher Al contents in the polymer matrix. Electrical and thermal conductivity values of HDPE-Al composites were higher than pure HDPE values.     

Preparation and Dynamic Tensile Behavior of C200 Green Reactive Powder Concrete

A new type of green reactive powder concrete (GRPC) with compressive strength of 200 MPa is prepared by utilizing composite mineral admixtures, natural fine aggregates, and short and fine steel fibers. The quasi-static mechanical properties (mechanical strength, toughness, fracture energy and interfacial bonding strength) of GRPC specimens, cured in three different types of regimes, are investigated. The experimental results show that the mechanical properties of the C200 GRPC made with the powder binders that is composed of 40% of Portland cement, 25% of ultra fine slag, 25% of ultra fine fly ash and 10% of silica fume are better than the others'. The corresponding compressive strength, flexural strength and fracture energy are more than 200 MPa, and 30 000 J/ m2 respectively. The dynamic tensile behavior of the C200 GRPC is also investigated through the split Hopkinson pressure bar (SHPB) according to the spalling phenomenon. The dynamic testing results demonstrate that strain rate has an important effect on the dynamic tensile behavior of GRPC. With the increase of strain rate, its peak stress and relevant strain increase. The GRPC exhibits an excellent strain ratio stiffening effect under the dynamic tensile load with high strain ratio, resulting in a significant change of the fracture pattern.     

一种水性可剥离涂料的研制

某种液体橡胶可以作为水性可剥离涂料的成膜物质;该涂料适用范围广泛,可以从木材、钢铁、铝材、有机玻璃、聚乙烯、聚氯乙烯、玻璃等的表面顺利剥离;讨论了影响涂料性能的几个因素;该涂料涂膜的扯断强度大于15 Mpa,扯断伸长率约700%,撕裂强度约35KN/m.