微波辐射合成3-氨基-1,2,4-三氮唑

在微波辐射条件下,以氨基胍重碳酸盐和甲酸为原料合成了3-氨基-1,2,4-三氮唑,反应速度比传统加热条件提高300倍,产率达到83.5%。优化后的最佳反应条件为微波输出功率为120 W,氨基胍重碳酸盐:甲酸摩尔比为1:1.25,溶剂无水乙醇为5mL,反应时间为60 s。     

层析Al2O3循环利用方案

对用于柱色谱分离的填充材料Al2O3，采用清洗、过筛、调节pH值、净化、干燥和活化处理，对获得的Al2O3进行物理性状测试和柱色谱性能研究。结果发现经过煅烧和微波辐射的Al2O3物理性状符合实验要求，对靛酚和甲基橙分离性能良好，两者之间的比移值Rf范围在8．6～9．3，可以采用该工艺对Al2O3进行循环利用。     

镍-磷-氧化铁纳米复合材料镀层的制备及其性能研究

采用复合化学镀方法制备了镍-磷-氧化铁纳米复合材料镀层。通过孔隙率、耐腐蚀性、硬度、耐磨性等性质试验,结果表明:纳米复合镀层致密性、耐腐蚀性和耐磨性等均优于A3钢片,甚至优于Ni-P镀层。     

电导法测定醋酸在H2O和THF混合溶剂中的活度系数

用电导法测定了醋酸在不同温度时和不同浓度下在H2O和THF混合溶剂中的电导丰，应用Debye-Hucker和OsagerFalkenhangen公式计算了醋酸在混合溶剂中的活度系数。并讨论了温度和浓度对电解质活度系数的影响。结果表明。电解质溶液的活度系数随着温度的增加而增大，随着浓度的增加而减小。     

统计学中几个容易混淆的问题

统计学是一门重要的学科,在日常生活中有着极其广泛的应用。本文对统计学教学中几个容易混淆的问题进行阐明,旨在帮助学生对统计学中的一些概念有个正确的理解。     

基于P2P技术的网格资源管理方法

网格计算的关键技术是资源管理,如何有效地对网格资源进行管理调度是一个网格系统是否可用的关键问题。基于网格资源的特点,文本试图在网格环境中引入对等思想,利用P2P技术来有效地管理动态的网格计算资源。     

Hybrid ants-like search algorithms for P2P media streaming distribution in ad hoc networks

Media streaming delivery in wireless ad hoc networks is challenging due to the stringent resource restrictions,po-tential high loss rate and the decentralized architecture. To support long and high-quality streams,one viable approach is that a media stream is partitioned into segments,and then the segments are replicated in a network and served in a peer-to-peer(P2P) fashion. However,the searching strategy for segments is one key problem with the approach. This paper proposes a hybrid ants-like search algorithm(HASA) for P2P media streaming distribution in ad hoc networks. It takes the advantages of random walks and ants-like algorithms for searching in unstructured P2P networks,such as low transmitting latency,less jitter times,and low unnecessary traffic. We quantify the performance of our scheme in terms of response time,jitter times,and network messages for media streaming distribution. Simulation results showed that it can effectively improve the search efficiency for P2P media streaming distribution in ad hoc networks.     

对P2P技术传播涉及相关法律问题的分析

先简要介绍了一种新兴的互联网技术P2P技术的工作原理和应用,以及其带来的主要法律问题,然后结合全球首宗因P2P应用软件——BT下载侵权行为被法院裁定罪名成立的案例,分析其对现行版权制度的冲击和影响,提出保障其健康发展的法律建议。     

声波垂直入射在两种介质界面处的反射和透射

通过对入射波、反射波和透射波振幅和声压的定量比较，得到了声波垂直入射在分界面处位移和声压的反射系数和透射系数，并对各种情况下的反射波和透射波进行了分析讨论．     

Should Science be Taught in Early Childhood?

This essay considers the question of why we should teach science to K-2. After initial consideration of two traditional reasons for studying science, six assertions supporting the idea that even small children should be exposed to science are given. These are, in order: (1) Children naturally enjoy observing and thinking about nature. (2) Exposing students to science develops positive attitudes towards science. (3) Early exposure to scientific phenomena leads to better understanding of the scientific concepts studied later in a formal way. (4) The use of scientifically informed language at an early age influences the eventual development of scientific concepts. (5) Children can understand scientific concepts and reason scientifically. (6) Science is an efficient means for developing scientific thinking. Concrete illustrations of some of the ideas discussed in this essay, particularly, how language and prior knowledge may influence the development of scientific concepts, are then provided. The essay concludes by emphasizing that there is a window of opportunity that educators should exploit by presenting science as part of the curriculum in both kindergarten and the first years of primary school.