锌基铝铜合金中铁和铜的测定

锌基铝铜合金试样用硝酸溶解,其中铁的测定是移取0．05g试样液,用盐羟胺将Fe^3 还原为Fe^2 ,于PH4-5时,Fe^2 与邻二氮菲生成红色络合物．为消除基体Zn及大量铜的干扰,采用加过量的邻二氮菲及延长显色时间,得到了准确的分析结果。铜的测定采用新铜试剂及DDTC-Pb两种方法对照分析试验,在本试验确定的条件下分析标样,得到准确结果。标样分析选取率为100%。测定范围：Fe0．01～0．1%;铜0．1～3．0%。通过标样定位分析结果表明本试验所确定的分析方法具有准确度高、灵敏度适宜、重现性好,能满足锌基铝铜合金产品分析的需要．     

难加工材料的切削加工及刀具材料的选用

随着科学技术的发展和机加工工艺水平的提高,不锈钢、淬火钢、高温合金钢等特殊材料在生产中的应用越来越广泛。难加工材料的切削加工效果与切削刀具材料的合理选用有着密切的关系。正确选用合适的切削刀具材料,合理选择加工规范,对提高工作效率,改善加工工艺性,更好的适应机械制造生产需求具有重要的意义。     

High-entropy-alloy nanoparticles with 21 ultra-mixed elements for efficient photothermal conversionOA

Multi-metallic nanoparticles have been proven to be an efficient photothermal conversion material, for which the optical absorption can be broadened through the interband transitions(IBTs), but it remains a challenge due to the strong immiscibility among the repelling combinations. Here, assisted by an extremely high evaporation temperature, ultra-fast cooling and vapor-pressure strategy, the arc-discharged plasma method was employed to synthesize ultra-mixed multi-metallic nanoparticles compose...     

铝合金压铸模具温度场数值分析

采用PROCAST对铝合金压铸用模具在压铸过程中的温度场进行了数值模拟,对压铸边界条件和传热系统的潜热采用热焓法进行了处理,分析了在不同时刻模具的温度场分布,分析了在不同的浇注温度和不同的模具预热温度情况下对模具温度场的影响,并且预测了热应力集中的位置,对压铸工艺参数的优化提出了见解,分析了冷却水管的作用,为压铸模具的热应力分析奠定基础。     

铸造高温合金K423A的切削加工性能研究

对铸造高温合金的切削加工进行了分析,重点对K423A的材料特点和加工性能进行了分析,并对其切削加工的条件从刀具材料、几何参数、切削用量的选择等方面进行了研究。     

浓硫酸法从废钨铜合金中回收金属钨和铜

本文介绍了用热的浓硫酸处理为钨铜合金，回收金属钨和铜的方法。     

Investigation on hot deformation behavior of AZ31 magnesium alloy

Magnesium and magnesium alloys, which have a density of 1.74 g cm-3, are the lightest structural metal. In addition to being extremely light, magnesium alloys have many advantages such as high specific strength and high specific rigidity [1-3]. Magnesium alloys have been paid more and more attention in recent years. A few die castings of magnesium alloys have been applied to automobile industry. Magnesium alloys have huge potentiality of application to automobile, motorcycle, aviation, spacefl…     

Durability of Bridge Expansion Joints with Perforated Dowels Under Traffic Impact Loading

In design phases, expansion joints are required to have movement capacity, bearing capacity for static and dynamic loading, watertight, low noise emission and traffic safety. On the basis of the fact that failure due to dynamic loading is the main reason for the observed damages, attention is focused on the bearing capacity for dynamic loading governed by impact, because it differs from the static loading. In this study, from the viewpoint of durability, experimental studies for. dynamic behavior were conducted for aluminium alloy expansion joints with perforated dowels. The validity of the perforated dowels against traffic impact loading was confirmed by both experimental and numerical studies.     

等离子体喷涂铁合金涂层缺陷回复行为的正电子寿命谱

用正电子湮没寿命谱方法结合硬度测试手段,对等离子体喷涂铁合金涂层退火处理后的微观结构及缺陷进行了研究,讨论了不同退火温度下缺陷的回复行为,提出退火回复的主要机制。     

非晶态Co（Ni）－B合金催化剂的TPD－MS研究

用化学还原法制备了非晶态合金催化剂Ｎｉ－Ｂ、Ｃｏ－Ｂ和Ｃｏ－Ｎｉ－Ｂ．合金的非晶性质由Ｘ射线衍射（ＸＲＤ）及透射电子显微镜（ＴＥＭ）鉴定．组成用电感耦合等离子发射光谱（ＩＣＰ）分析．在高真空程序升温脱附质谱（ＴＰＤ－ＭＳ）装置上研究了ＣＯ、Ｈ２在三种催化剂上的吸附及ＣＯ和Ｈ２的表面反应（ＴＰＳＲ）．发现ＣＯ和Ｈ２在三种催化剂上分别有二种和一种吸附态，吸附强度和二种吸附态的数目在不同合金上有较大差异．ＣＯ加氢反应的主要产物是ＣＨ４、ＣＯ２和Ｈ２Ｏ，其中ＣＯ在催化剂表面上的解离是反应的控制步骤．