低应变法检测桥梁嵌岩桩的评价

用低应变法检测嵌岩桩 ,若桩底出现明显同相反射 ,多数因桩底缺陷引起。而区分是桩还是持力层的缺陷 ,主要看反射的起跳时间在 2 L/ C之前还是之后。当桩的变径及入岩反射对测试影响很大时 ,应进一步用钻芯法检验。     

Technical analysis of a Central Asian wall painting detached from a Buddhist cave temple on the northern Silk Road

A great number of Central Asian wall paintings, archeological materials, architectural fragments, and textiles, as well as painting fragments on silk and paper, make up the so called Turfan Collection at the Asian Art Museum in Berlin. The largest part of the collection comes from the Kucha region, a very important cultural center in the third to ninth centuries. Between 1902 and 1914, four German expeditions traveled along the northern Silk Road. During these expeditions, wall paintings were detached from their original settings in Buddhist cave complexes. This paper reports a technical study of a wall painting, existing in eight fragments, from the Buddhist cave no. 40 (Ritterhöhle). Its original painted surface is soot blackened and largely illegible. Grünwedel, leader of the first and third expeditions, described the almost complete destruction of the rediscovered temple complex and evidence of fire damage. The aim of this case study is to identify the materials used for the wall paintings. Furthermore, soot deposits as well as materials from conservation interventions were of interest. Non-invasive analyses were preferred but a limited number of samples were taken to provide more precise information on the painting technique. By employing optical and scanning electron microscopy, energy dispersive X-ray spectroscopy, micro X-ray fluorescence spectroscopy, X-ray diffraction analysis, and Raman spectroscopy, a layer sequence of earthen render, a ground layer made of gypsum, and a paint layer containing a variety of inorganic pigments were identified.     

太赫兹时域光谱技术

介绍了太赫兹时域光谱技术的优势,太赫兹时域光谱系统及太赫兹时域光谱技术的原理和应用.     

Case Report:Lance-Adams syndrome:a report of two cases

Chronic post-hypoxic myoclonus, also known as Lance-Adams syndrome (LAS), is a rare complication of successful cardiopulmanry resuscitation often accompanied by action myoclonus and cerebellar ataxia. It is seen in patients who have un-dergone a cardiorespiratory arrest, regained consciousness afterwards, and then developed myoclonus days or weeks after the event. Worldwide, 122 cases have been reported in the literature so far, including 1 case of Chinese. Here we report 2 Chinese LAS patients with detailed neuroimagings. Cranial single photon emission computed tomography (SPECT) of patient 1, a 52-year-old woman, showed a mild hypoperfusion in her left temporal lobe, whereas patient 2, a 54-year-old woman, manifested a mild bilateral decrease of glucose metabolism in the frontal lobes and a mild to moderate decrease of the N-acetyl aspartate (NAA) peak in the bilateral hippocampi by cranial [18F]-fluorodeoxyglucose positron emission tomographic (PET) scan and cranial magnetic resonance spectroscopy (MRS), respectively. We also review the literature on the neuroimaging, pathogenesis, and treatment of LAS.     

实验教材中“荧光光谱法测定水杨酸”的讨论

为改进教材《荧光光谱法测定水杨酸》,寻找实验所需溶剂CHCl3的替代药品。通过实验,采用1%HAc-CHCl3、1%HAc-C2H5OH、1%HAc-H2O对荧光光谱法测定水杨酸的影响进行比较,并确定1%HAc-C2H5OH为其中最佳溶剂。     

A highly alkaline-stable metal oxide@metal–organic framework composite for high-performance electrochemical energy storage

Most metal–organic frameworks (MOFs) hardly maintain their physical and chemical properties after exposure to alkaline aqueous solutions, thus precluding their use as potential electrode materials for electrochemical energy storage devices. Here, we present the design and synthesis of a highly alkaline-stable metal oxide@MOF composite, Co₃O₄ nanocube@Co-MOF (Co₃O₄@Co-MOF), via a controllable and facile one-pot hydrothermal method under highly alkaline conditions. The obtained composite possesses exceptional alkaline stability, retaining its original structure in 3.0 M KOH for at least 15 days. Benefitting from the exceptional alkaline stability, unique structure, and larger surface area, the Co₃O₄@Co-MOF composite shows a specific capacitance as high as 1020 F g⁻¹ at 0.5 A  g⁻¹ and a high cycling stability with only 3.3% decay after 5000 cycles at 5 A g⁻¹. The as-constructed solid-state flexible device exhibits a maximum energy density of 21.6 mWh cm⁻³.     

Study of the stability of a series of synthetic colorants applied with styrene-acrylic copolymer, widely used in contemporary paintings, concerning the effects of accelerated ageing

This study examines the materials of a contemporary pictorial artwork, belonging to the Macedonian Museum of Contemporary Art in Thessaloniki (Greece), and needing conservation. The combined use of micro-FTIR and micro-Raman spectroscopy allowed the identification of almost all painting materials. Moreover, the stability of a series of synthetic pigments towards accelerated ageing is investigated in applications using the contemporary binding medium styrene-acrylic copolymer. The pigments in question are: Hansa yellow PY3 and PY74, quinacridone PV19 and PR122, naphthol AS PR112, phthalocyanine green PG7 and blue PB15, dioxazine PV37, van Dyck brown PBk11, ivory black PBk9, and titanium dioxide PW6. The organic pigments were applied alone or mixed with titanium dioxide, in rutile form or as a mixture of rutile/anatase. The experimental swatches were subjected to ageing tests, and subsequently studied as to colour changes by means of colorimetric measurements, and as to the molecular structure differentiations by infrared spectroscopy in reflectance mode. The ageing tests included exposure to high temperature and humidity (90 °C, 60% RH) and to ultraviolet radiation (350 nm, 30 °C and 50% RH, with a substantial temperature increase at 90 °C for 3 days). The greater colour difference is caused by high temperature and humidity, whereas paint layers containing TiO₂, and especially the mixture of the forms rutile/anatase, prove very susceptible to ultraviolet radiation, demonstrating a significant colour difference and extended molecular changes.     

船闸阻抗影响下的内河航线非线性配船模型

为得到可靠的最优航线配船方案,从内河繁忙航线上船舶过闸的时间开始研究,得出船舶经过船闸处时间变动与航线配船数量的关系;在线性规划的航线配船模型基础上,建立受船闸时间阻抗变动影响的航线非线性配船模型.应用该模型,设计某一内河航运船队的最优配船方案.分析表明,该非线性模型考虑的影响因素更全面,运用该模型得到的配船结果比线性规划模型更合理.     

20-69周岁年龄人群体脂分布情况的研究

为了解20--69周岁年龄人群体脂分布情况,本研究随机抽取了浙江省25个县、区的城乡居民,共2775人,女性1449人,男性1326人。依据《2005年国民体质监测工作手册》的要求,10岁为一个年龄组,共分20-29周岁、30～39周岁、40～49周岁、50-59周岁和60～69周岁5个纽别,并采用日本TANITA多频身体成分分析仪（MC-180）对人体进行身体成分的测试,结果显示：①体脂量和体脂百分比女性呈持续上升,男性为先上升后下降;②体脂量的增加主要有表现在躯干部位脂肪含量的增加,躯干成为脂肪堆积主要部位;③内脏脂肪含量增加幅度最大,男性约增加73．42％,女性约增加150．91％。     

一种DDR信号阻抗匹配的新方法

DDR信号的阻抗匹配一般有两种方法:源端增加串联电阻和终端增加并联电阻。这两种方法各有利弊。其中源端串阻匹配会增加单板PCB的布板面积,终端并联匹配则会增加单板的功耗。本文则采用并联电容来替代并联电阻,这样即可以解决PCB布板面积的问题,也可以解决单板机功耗增加的问题,是DDR信号匹配的一种新方法。