硫酸铁铵对安息香的氧化

将安息香与十二水合硫酸铁铵在稀醋酸中回流70min得苯偶酰,收率86％～95％．     

阴离子淀粉研究进展

文章论述了阴离子淀粉的分类、性质、制备、应用以及发展前景,展望了该产品的研究方向及其潜在的应用领域。     

硫酸复盐法回收NdFeB废料中含铁水的处理

采用化学手段,对硫酸复盐法回收钕铁硼废料时产生的含铁废水进行处理。通过对钕铁硼废料进行充分的焙烧,使铁、钕均转化为氧化物。再经酸解、溶解后趁热过滤,通过结晶,重结晶,烘干得到硫酸亚铁盐。实验中得到的硫酸亚铁纯度达到了81.35%。该实验方式不仅可得到钕铁硼磁体废料中的稀土金属（氧化物）,同时回收了大量的含铁盐,而且还减少了对环境的污染,是对硫酸复盐法的补充,因此在实际生产中会得到良好的应用。     

盐析法沉淀柠檬皮果胶简

以柠檬皮为原料,采用酸水解盐析法对柠檬果胶的沉淀工艺进行研究.通过单因素法分析沉淀果胶的硫酸锌用量、盐析pH、温度、时间等影响因素,然后正交实验法优化盐析法沉淀柠檬皮果胶的最佳工艺.实验结果表明：以上因素都有影响,其中沉淀剂量影响最大.最佳工艺条件为硫酸锌用量为干柠檬皮质量的0.3倍,盐析pH为5.0,盐析温度为45℃,盐析时间为120 min.通过上述条件得到较好性状的浅黄颗粒状产品,果胶提取率为18.72％.     

离子色谱法测定铝箔腐蚀液中硫酸根

建立了用阳离子交换树脂去除铝离子,然后用离子色谱法测定铝箔腐蚀液中硫酸根的方法.酸性条件下,阳离子交换树脂能够将铝箔腐蚀液中的Al3 全部除去;阳离子交换树脂不会吸附待测的阴离子;用离子色谱测定铝箔腐蚀液中SO42-可行,回收率93.81%~99.87%.样品处理的效果好,测定结果令人满意.     

硫酸锰溶液多效蒸发新工艺研究

采用多效蒸发方法,对硫酸锰溶液的预浓缩工艺进行了研究。实验通过考察进料浓度,蒸发温度,一效、二效蒸发真空度对蒸发水量的影响。结果表明,进料的浓度越低,蒸发效率越高,蒸发的温度越高,蒸发效率越高,强制搅拌越大,蒸发效果越好,降低一效、二效的蒸发真空度,可有效抑制结晶的析出,减少结垢对蒸发效率的影响。该工艺对开发节能降耗生产硫酸锰的新工艺都具有重要的指导意义。     

Molecular mechanism of pathogenesis of dengue virus: Entry and fusion with target cell

Dengue fever is one of the major health problems in India. Interaction with specific receptor(s) at the cell surface is one of the first events in the pathogenesis of Dengue virus. However, relatively little is known about these receptors. Cellular receptors in human monocytes and mouse neural cells are main target for the viral infection. The envelope protein of the virus (E-protein) plays important role in attachment of virus to target cells and their interaction with cellular receptors. The modulation of receptor gene(s) and/or protein(s) can be used as a method for interfering with virus entry and can thus become a new method for disease prevention. The receptors can be purified by affinity chromatography using E-protein as ligand. It has been reported that addition of highly sulfated heparan sulfate prevents E-protein binding to target cells suggesting that heparan sulfate is utilized by dengue envelope protein to bind to target cells.     

无水硫酸铁及球型干燥剂的制备

无水硫酸铁的干燥强度优于无水硫酸镁 ;干燥容量大大超过硅胶 ,是很值得开发的一种无机盐干燥剂 .由硫铁矿烧渣制备硫酸铁并将其制成球型 ,不仅降低了成本 ,而且使用方便 .这种造粒方法原则上也适用于其它常用的无机盐干燥剂     

硫酸铝渣作混合材对水泥性能影响的研究

生产硫酸铝排出的尾渣,是一种具有富含活性SiO2的人工火山灰材料,部分替代矿渣作水泥混合材,可以明显缩短水泥凝结时间,提高水泥28d强度,但标准稠度需水量明显增加。适当提高熟料矿物组成中C3A的比例,或掺加适量石灰石作混合材,以及对硫酸铝渣进行粉磨预处理等措施,对水泥性能的影响值得进一步研究。     

Individual and joint toxic effects of cadmium sulfate and α-naphthoflavone on the development of zebrafish embryo

This paper aims to evaluate the individual and joint toxicities of cadmium sulfate (CdSO₄) and α-naphthoflavone (ANF) in zebrafish embryos. As a result, CdSO₄ caused both lethal and sub-lethal effects, such as 24 h post-fertilization (hpf) death and 72 hpf delayed hatching. However, ANF only caused sub-lethal effects, including 48 hpf cardiac edema and 72 hpf delayed hatching. Taking 24 hpf death and 48 hpf cardiac edema as endpoints, the toxicities of CdSO₄ and ANF were significantly enhanced by each other. Consistently, both CdSO₄ and ANF caused significant oxidative stress, including decreases in the reduced glutathione (GSH) level, inhibition of superoxide dismutase (SOD) activity, as well as increases in malondialdehyde (MDA) content in zebrafish embryos, but these mixtures produced much more significant alterations on the biomarkers. Co-treatment of CdSO₄ and ANF significantly down-regulated the mRNA level of multidrug resistance-associated protein (mrp) 1 and cytochrome P450 (cyp) 1a, which constituted the protective mechanisms for zebrafish embryos to chemical toxins. In conclusion, co-treatment of CdSO₄ and ANF exhibited a much more severe damage in zebrafish embryos than individual treatment. Meanwhile, production of oxidative stress and altered expression of mrp1 and cyp1a could be important components of such joint toxicity.