Preanalytical phase--a continuous challenge for laboratory professionals

Preanalytical phase is the most vulnerable part of the total testing process and is considered to be among the greatest challenges to the laboratory professionals. However, preanalytical activities, management of unsuitable specimens and reporting policies are not fully standardized, nor harmonized worldwide. Several standards related to blood sampling and sample transportation and handling are available, but compliance to those guidelines is low, especially outside the laboratory and if blood sampling is done without the direct supervision of the laboratory staff. Furthermore, for some most critical procedures within the preanalytical phase, internationally accepted guidelines and recommendations as well as related quality measures are unfortunately unavailable. There is large heterogeneity in the criteria for sample rejection, the different strategies by which unacceptable samples are managed, processed and test results reported worldwide. Management of unacceptable specimens warrants therefore immediate harmonization. Alongside the challenging and long road of patient safety, preanalytical phase offers room for improvement, and Editors at Biochemia Medica Journal definitely hope to continue providing a respective mean for reporting studies on different preanalytical phase topics. With pleasure and delight we invite potential future authors to submit their articles examining the quality of various preanalytical activities to Biochemia Medica. We will keep nurturing this topic as our prominent feature and by this we hope to be able to deliver valid evidence for some future guidelines and recommendations.     

固相萃取-气相色谱质谱法测定水中七氯

实验采用固相萃取-气相色谱质谱法对水样的七氯进行分析,优化前处理条件及气相色谱质谱条件,方法最低检测质量浓度可达0.00005mg/L,标准曲线的线性相关系数r2=0.998线性范围为0.0002～0.01mg/L,样品平均加标回收率在101.7%～112.4%之间,相对标准偏差在1.81%～5.15%。该方法操作简单、灵敏度高、准确、重现性好。     

硬脂酸十六烷酯的合成与相变储能性能研究

通过羧基酰氯酯化法合成了硬脂酸十六烷酯固—液相变材料,并使用傅立叶红外光谱仪（FT-IR）、广角X-射线衍射仪（WAXD）、示差扫描量热仪（DSC）、热重分析仪（TG）等测试手段研究了材料的结构、结晶性能以及热性能（相变焓、相变温度和热稳定性）,发现所得材料具有较高的焓变,同时其热稳定性相比硬脂酸和十六醇得到了较大的提高,是一种具有较好相变性能的新型固—液相变储能材料.     

毛泽东对社会主义发展阶段的探索及其当代意义

建国以后,我国处于什么发展阶段,采取什么方式和手段巩固和发展社会主义,毛泽东和中共党人进行了艰辛探索,形成了马克思主义中国化的重要理论成果。毛泽东探索社会主义发展阶段的理论基础和思想认识是马克思主义的“不断革命论”“革命发展阶段论”和科学社会主义理论,具有伟大的当代意义。     

利用超导量子干涉仪制备N比特团簇态

利用两个超导量子干涉仪与腔场的相互作用,提出一种实现标准两比特量子相位门的方案.利用构造的两比特相位门,还提出了一种制备N比特团簇态的方案.在此方案中,量子信息被编码在两个超导量子干涉仪的相对稳定的基态上.在两个超导量子干涉仪与单模腔场的相互作用过程中,由于超导量子干涉比特的激发态被绝热地消去,激发态所引起的消相干得到了有效的抑制.此外,还讨论方案的实验可行性.     

四氧化三锰的简易制备

在90℃水浴加热条件下,采用空气氧化法于弱碱性介质中氧化Mn^2＋制备四氧化三锰.研究了MnCl2起始浓度、MnCl2和六次甲基四胺的配比、溶液极性对反应产物晶型和形貌的影响.所得产物进行X-射线衍射和扫描电镜表征.结果表明,不同条件下所得产物均为四氧化三锰,而且纯度高、结晶良好,呈球状.     

AlN/ZL101原位复合材料的正交实验研究

通过正交实验分析,利用气液反应法制备原位AlN/ZL101复合材料并确定了其最佳成分,测试了复合材料的力学性能并对该材料进行了显微金相分析和透射电子显微分析。研究结果表明:AlN/ZL101原位复合材料中原位生成增强体AlN的尺寸为30nm左右,均匀分布于共晶体内部,同基体结合良好;由于细小增强相的作用,热处理后复合材料中的共晶硅以粒状形态均匀分布于基体中。     

信息服务的趋同与转型

随着数字信息技术的普及,信息服务开始向数字化、网络化和综合化转型。信息服务机构之间不再以信息生产、存储和传播技术为边界,而以不同的用户和市场为边界,跨行业竞争与合作,为各自的用户提供多媒体信息服务和综合信息服务。     

The role of school leadership in the implementation of the Transition Year Programme in Ireland

Introducing an educational innovation into any school context involves some challenge to existing practices. Transition Year is an innovative, optional, one-year programme taken by approximately half the 15–16-year age cohort in schools in the Republic of Ireland. Based on data from an extensive study of TY operating in six different schools, programme co-ordinators and school principals are identified as having key roles in the successful implementation of TY. However, exercising the collegiality both roles demand goes against established cultures of isolated individualism in Irish schools. Furthermore, maintaining TY's coherence and integrity in the face of threats from more established programmes offers particular challenges. For this innovation to be successful, active curriculum leadership by school principals is seen as crucial. The paper interrogates the evidence through the lens of the 2008 OECD study on school leadership and poses questions about the relevance and value of the OECD perspective.     

讨论光的干涉和衍射问题时引入光程差概念的物理意义

本文主要论述结合光的干涉,衍射现象的本质,讨论引入光程差概念的物理意义,从波动性概念解释光的干涉和衍射现象的本质,最后得到光程差概念的物理意义。