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排序方式: 共有489条查询结果,搜索用时 78 毫秒
1.
介绍一种基于红外成像技术的金属焊接质量的无损检测方法.首先介绍了检测的基本原理和检测装置,然后详细给出了以边缘检测为基础的缺陷检测方法及检测结果.最后通过比较说明,利用红外成像技术对金属焊接质量进行无损检测是一种很有效的方法. 相似文献
2.
A multi-analytical approach for the study of brazilwood and its lake pigments was carried out based on historically accurate reconstructions. Recipes for brazilwood lakes from the fifteenth century technical text Livro de como se fazem as cores and the Winsor & Newton nineteenth century colourman's archive were reproduced and compared. Both primary sources allowed for the successful preparation of brazilwood lake pigments with colours that vary from light pink to dark red. The main steps and ingredients for the manufacture of these pigments were common in both sources, particularly the addition of Al3+ in the form of alum, and calcium carbonate (chalk). Reconstructions revealed that the latter acts as a pH buffer and filler, controlling the pH at which the lake pigment precipitates. The main difference between the two sources is that the nineteenth century recipes give the quantities for all ingredients, the precise temperatures and time, and achieved higher relative pigment yields (75% versus 45%). Full chemical characterisation of the reconstructions provided detailed information on the individual steps in the pigment manufacture and revealed that the presence of calcium sulphate dihydrate (gypsum) in the final pigment was a result of its formation in situ. Infrared, reflectance, and fluorescence spectroscopy proved to be essential and complementary techniques: while infrared was used to characterise additives and binders, reflectance and fluorescence data were fundamental for identifying the chromophore. The pigments and paints produced can now be used as standards for the identification and investigation of brazilwood lake pigments found in artworks. 相似文献
3.
Birgit Angelika Schmidt Martin Andreas Ziemann Simone Pentzien Toralf Gabsch Werner Koch Jörg Krüger 《文物保护研究》2016,61(2):113-122
A great number of Central Asian wall paintings, archeological materials, architectural fragments, and textiles, as well as painting fragments on silk and paper, make up the so called Turfan Collection at the Asian Art Museum in Berlin. The largest part of the collection comes from the Kucha region, a very important cultural center in the third to ninth centuries. Between 1902 and 1914, four German expeditions traveled along the northern Silk Road. During these expeditions, wall paintings were detached from their original settings in Buddhist cave complexes. This paper reports a technical study of a wall painting, existing in eight fragments, from the Buddhist cave no. 40 (Ritterhöhle). Its original painted surface is soot blackened and largely illegible. Grünwedel, leader of the first and third expeditions, described the almost complete destruction of the rediscovered temple complex and evidence of fire damage. The aim of this case study is to identify the materials used for the wall paintings. Furthermore, soot deposits as well as materials from conservation interventions were of interest. Non-invasive analyses were preferred but a limited number of samples were taken to provide more precise information on the painting technique. By employing optical and scanning electron microscopy, energy dispersive X-ray spectroscopy, micro X-ray fluorescence spectroscopy, X-ray diffraction analysis, and Raman spectroscopy, a layer sequence of earthen render, a ground layer made of gypsum, and a paint layer containing a variety of inorganic pigments were identified. 相似文献
4.
Jiří Baláš David Giles Jan Kodejška Michaela Panáčková Simon Fryer 《European Journal of Sport Science》2016,16(7):764-772
This study aimed to (1) evaluate the effect of hand shaking during recovery phases of intermittent testing on the time–force characteristics of performance and muscle oxygenation, and (2) assess inter-individual variability in the time to achieve the target force during intermittent testing in rock climbers. Twenty-two participants undertook three finger flexor endurance tests at 60% of their maximal voluntary contraction until failure. Performances of a sustained contraction and two intermittent contractions, each with different recovery strategies, were analysed by time–force parameters and near-infrared spectroscopy. Recovery with shaking of the forearm beside the body led to a significantly greater intermittent test time (↑ 22%, P?.05), force–time integral (↑ 28%, P?.05) and faster muscle re-oxygenation (↑ 32%, P?.05), when compared to the hand over hold condition. Further, the ratio of intermittent to continuous test time distinguished specific aerobic muscular adaptations among sport climbers (2.02), boulderers (1.74) and lower grade climbers (1.25). Lower grade climbers and boulderers produced shorter duration contractions due to the slower development of target force during the intermittent test, indicating worse kinaesthetic differentiation. Both the type of recovery and climbing discipline determined muscle re-oxygenation and intermittent performance in rock climbers. 相似文献
6.
水杨酸铁的流变相合成和红外光谱 总被引:1,自引:0,他引:1
用流变相反应法合成了水杨酸铁配合物,对样品在4000—400cm^-1。范围内的主要红外光谱吸收峰进行了归属,通过元素分析、TG和IR确定该配合物的组成为Fe(HSal)3.3H2O(HSal=O-OHC6H4CO2)。 相似文献
7.
LU Bao - qi 《上海大学学报(英文版)》2005,9(4):365-368
Infrared (IR) absorption spectra and X-ray powder diffraction (XRD) patterrns of sexpenfine cat's eye from Sichuan Province have been investigated, and infrared absorption bands of the serpentine have been assigned in this paper. The results indicate that the bands near 3 600 - 3 700 cm^-1 belong to the stretching absorption band VOH, the bands in 948 - 1 100 cm^-1 axe assigned to the stretching vibraling band Usvo, and the bands at 600 570 and 440 cm^-1 respectively belong to the bending vibration band VOH, δMg-O and δSi-O. The serpentine cat' s eye includes two types: chrysotile and antigorite. Chrysotile has a sharp and intensive band at 3 688 cm^-1 and a weak band at 3 643 cm^-1 , while antigorite has only one intensive band in the region. At vibration band VSi-O, chrysotile and antigorite have a similar feature at 1 071 cm^-1, but the band at 980 cm^-1 in anfigorite has been split into two bands in chrysotile - a strong one at 1 027 cm^-1 and a weak one at 949 cm^-1. In addition, antigorite has a characteristic bending vibrating band δMg-O at 570 cm^-1. Based on the analysis of the feature of crystal structure, their IR differences axe well explained. 相似文献
8.
ZHANG Yan-xing LIU Jian-ren JIANG biao LIU Hui-qin DING Mei-ping SONG Shui-jiang ZHANG Bao-rong ZHANG Hong XU Bin CHEN Huai-hong WANG Zhong-jin HUANG Jian-zheng 《Journal of Zhejiang University. Science. B》2007,(10)
Chronic post-hypoxic myoclonus, also known as Lance-Adams syndrome (LAS), is a rare complication of successful cardiopulmanry resuscitation often accompanied by action myoclonus and cerebellar ataxia. It is seen in patients who have un-dergone a cardiorespiratory arrest, regained consciousness afterwards, and then developed myoclonus days or weeks after the event. Worldwide, 122 cases have been reported in the literature so far, including 1 case of Chinese. Here we report 2 Chinese LAS patients with detailed neuroimagings. Cranial single photon emission computed tomography (SPECT) of patient 1, a 52-year-old woman, showed a mild hypoperfusion in her left temporal lobe, whereas patient 2, a 54-year-old woman, manifested a mild bilateral decrease of glucose metabolism in the frontal lobes and a mild to moderate decrease of the N-acetyl aspartate (NAA) peak in the bilateral hippocampi by cranial [18F]-fluorodeoxyglucose positron emission tomographic (PET) scan and cranial magnetic resonance spectroscopy (MRS), respectively. We also review the literature on the neuroimaging, pathogenesis, and treatment of LAS. 相似文献
9.
为改进教材《荧光光谱法测定水杨酸》,寻找实验所需溶剂CHCl3的替代药品。通过实验,采用1%HAc-CHCl3、1%HAc-C2H5OH、1%HAc-H2O对荧光光谱法测定水杨酸的影响进行比较,并确定1%HAc-C2H5OH为其中最佳溶剂。 相似文献
10.
讨论了氢原子光谱实验中狭缝宽度、采集次数和负高压对氢原子光谱同位素位移谱线的影响,优化了氢原子光谱同位素位移实验的工作参数,获得了清晰的氢原子同位素位移光谱。通过该实验让学生掌握实验中多参数优化的方法,有利于加深学生对光谱理论的理解,有利于提高学生分析问题解决问题的能力。 相似文献