排序方式: 共有25条查询结果,搜索用时 15 毫秒
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研究了XAD-4大孔树脂对水相中邻氨基苯酚的吸附特性。研究内容包括接触时间、pH、吸附剂质量、吸附温度对吸附的影响。树脂能有效地除去水相中的邻氨基苯酚,在pH=3.2~5.2的范围内树脂对邻氨基苯酚均有较大的吸附,其最佳酸度为pH=4.0,吸附率可达97.3%。研究表明Langmuir等温吸附模型能较好地描述吸附过程。用1.5~2.0 mol/L HCl对吸附后的树脂进行再生试验,脱附率可达91.2%。 相似文献
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以D-101树脂为吸附材料,研究不同条件下对蛇莓果实红色素的吸附和解吸性能.研究发现:静态吸附中上样液温度为30℃时的吸附量较大;动态吸附中上样液酸度为0.5%,吸光度0.179~0.224, pH1.0,流速2 mL/min时的吸附量大;用80%乙醇以2 mL/min的流速进行洗脱时,解吸效果最好;蛇莓果实色素纯化后色价提高了3倍左右,该研究条件科学合理,纯化效果很好. 相似文献
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介绍了一些干燥相关物理量的研究方法,并对微孔硅酸钙的干燥相关物理量进行了初步的研究.根据电子扫描电镜的成象分析,获得了该种材料内部结构的固有规律,并在此基础上通过理论分析和一些简单的实验相结合的方法,得到了诸如微孔硅酸钙的多孔率、毛细压力和解吸等温线等物理量,为进一步深入研究微孔硅酸钙的干燥特性提供了依据. 相似文献
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对含金4-5g/kg、含银7g/kg的负载炭用碱性醇溶液进行解吸,金银的解吸率都能达到98%以上,解吸液用电解槽进行电沉积,金的电解率达99%以上,银的电解率达98%以上。电积到钢棉上的金银泥用化学方法进行分离,金泥经熔炼后得合质金,银泥熔炼后可得98%的银锭。 相似文献
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Preoperatively molecular staging with CM10 ProteinChip and SELDI-TOF-MS for colorectal cancer patients 总被引:8,自引:0,他引:8
Xu WH Chen YD Hu Y Yu JK Wu XG Jiang TJ Zheng S Zhang SZ 《Journal of Zhejiang University. Science. B》2006,7(3):235-240
Objectives: To detect the serum proteomic patterns by using SELDI-TOF-MS (surface enhanced laser desorption/ ionization-time of flight-mass spectrometry) technology and CM10 ProteinChip in colorectal cancer (CRC) patients, and to evaluate the significance of the proteomic patterns in the tumour staging of colorectal cancer. Methods: SELDI-TOF-MS and CM10 ProteinChip were used to detect the serum proteomic patterns of 76 patients with colorectal cancer, among them, 10 Stage Ⅰ, 19 Stage Ⅱ, 16 Stage Ⅲ and 31 Stage Ⅳ samples. Different stage models were developed and validated by support vector machines, disctiminant analysis and time-sequence analysis. Results: The Model Ⅰ formed by 6 protein peaks (m/z: 2759.58, 2964.66, 2048.01, 4795.90, 4139.77 and 37761.60) could be used to distinguish local CRC patients (Stage Ⅰ and Stage Ⅱ) from regional CRC patients (Stage Ⅲ) with an accuracy of 86.67% (39/45). The Model Ⅱ formed by 3 protein peaks (m/z: 6885.30, 2058.32 and 8567,75) could be used to distinguish locoregional CRC patients (Stage Ⅰ, Stage Ⅱ and Stage Ⅲ) from systematic CRC patients (Stage IV) With an accuracy of 75.00% (57/76). The Model Ⅲ could distinguish Stage Ⅰ from Stage Ⅱ with an accuracy of 86.21% (25/29). The Model Ⅳ could distinguish Stage Ⅰ from Stage Ⅲ with accuracy of 84.62% (22/26). The Model Ⅴ could distinguish Stage Ⅱ from Stage Ⅲ with accuracy of 85.71% (30/35). The Model Ⅵ could distinguish Stage Ⅱ from Stage Ⅳ with accuracy of 80.00% (40/50). The Model Ⅶ could distinguish Stage Ⅲ from Stage Ⅳ with accuracy of 78.72% (37/47). Different stage groups could be distinguished by the two-dimensional scattered spots figure obviously. Conclusion: This method showed great success in preoperatively determining the colorectal cancer stage of patients. 相似文献
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无机磷在白浆土中的吸附与解吸机制 总被引:5,自引:0,他引:5
本文主要研究了土壤中铁铝氧化物对白浆土的表层和白浆层的磷酸盐吸附与解吸的影响以及在吸附和解吸过程中无机磷的释放和形态转化机理。研究结果表明,铁铝氧化物对磷的吸附和解吸都有影响,其中无定形铝的影响更大一些,而且铁铝氧化物对吸附的影响程度超过有机质。磷被白浆土吸附后,火部分转变成铝磷(Al-P)和铁磷(Fe-P)。相对来说,铝对磷的吸附在快反应阶段强于慢反应阶段,铁则相反。把吸磷后的样品恒温静置,则Al-P逐渐向Fe-P和Ca-P转化。吸附磷解吸时,也是以Al-P为主。Fe-P是较好的“速效磷源”,而Al-P既是较好的“速效磷源”,也是很好的“缓效磷源”。 相似文献
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为给学校的教学、科研提供强有力的技术支撑,给地方经济提供更新更专业的技术服务,生物医学研究院公共技术平台在已拥有3台MALDI源生物质谱的基础上,通过整合该类仪器在相对分子质量测定、肽段测序、新蛋白分析、蛋白质鉴定、蛋白质翻译后修饰和定量分析等方面的应用,率先建立了基于MALDI源的生物质谱技术子平台。针对该子平台所涉及仪器的原理进行简单介绍,实验技术进行实例演示,仪器共享服务的规章制度进行说明。在此基础上,进一步完善了大型仪器设备共享系统,提高了大型仪器和优质资源的使用效率和效益,展示了该子平台在生物医学领域不可或缺的地位。 相似文献