| 电化学合成碘仿装置的改进及反应条件的探索 |
| |
| 引用本文： | 李英俊,孙淑琴,刘化毅,王辉,周晓霞,孙鹏.电化学合成碘仿装置的改进及反应条件的探索[J].实验技术与管理,2007,24(3):49-51. |
| |
| 作者姓名： | 李英俊 孙淑琴 刘化毅 王辉 周晓霞 孙鹏 |
| |
| 作者单位： | 辽宁师范大学,化学化工学院,辽宁,大连,116029 |
| |
| 摘 要： | 对电化学合成碘仿装置进行了改进,探索出了利用该装置合成碘仿的最佳反应条件。结果表明,新装置能够满足半微量有机化学实验的要求,碘仿的产率可达到54.9%。该装置具有实用性和推广价值。
|
| 关 键 词： | 装置 碘仿 电化学 合成 |
| 文章编号： | 1002-4956（2007）03-0049-03 |
| 收稿时间： | 2006-08-15 |
| 修稿时间： | 2006-11-08 |
The improvement of the device on synthesizing iodoform by electrochemistry method and the exploring of reaction conditions |
| |
| LI Ying-jun,SUN Shu-qin,LIU Hua-yi,WANG Hui,ZHOU Xiao-xia,SUN Peng.The improvement of the device on synthesizing iodoform by electrochemistry method and the exploring of reaction conditions[J].Experimental Technology and Management,2007,24(3):49-51. |
| |
| Authors: | LI Ying-jun SUN Shu-qin LIU Hua-yi WANG Hui ZHOU Xiao-xia SUN Peng |
| |
| Institution: | College of Chemistry and Chemical Engineering, Liaoning Normal University, Liaoning Dalian 116029, China |
| |
| Abstract: | In this paper,a new device of synthesizing iodoform by electrochemistry method was introduced and the optimum reaction condition of synthesizing iodoform had been explored by this device.The results showed that the device could satisfy the requirments of the semi-microorganic chemistry experiment and the yield of iodoform reach 54.9%.The device possesses practicability and value of popularization. |
| |
| Keywords: | device iodoform electrochemistry synthesis |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
