| 三维网状超分子化合物树脂制备的最佳工艺条件确定 |
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| 引用本文： | 战佩英,李桂娟.三维网状超分子化合物树脂制备的最佳工艺条件确定[J].通化师范学院学报,2011,32(6):34-37. |
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| 作者姓名： | 战佩英 李桂娟 |
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| 作者单位： | 1. 通化师范学院化学系,吉林通化,134002
2. 长春工业大学化学工程学院,吉林长春,130012 |
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| 摘 要： | 针对传统吸附树脂在中药有效成分提纯中存在的不足,研究和制备了一种选择性高、具有筛分作用的三维网状超分子化合物树脂.通过对各种影响因素的对比分析,确定了制备树脂的最佳工艺条件：以碳酸钙为成孔剂,NaOH的浓度为20%,温度在50～55℃之间,交联剂用量15%,反应时间20min.
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| 关 键 词： | 树脂 成孔剂 β-环糊精 |
The Optimum Preparation of Three-dimensional Netlike Supramolecular Compound Resin |
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| ZHAN Pei-ying,LI Gui-juan.The Optimum Preparation of Three-dimensional Netlike Supramolecular Compound Resin[J].Journal of Tonghua Teachers College,2011,32(6):34-37. |
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| Authors: | ZHAN Pei-ying LI Gui-juan |
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| Institution: | ZHAN Pei-ying1,LI Gui-juan2(1.Department of Chemistry,Tonghua Normal University,Tonghua,Jilin 134002,China,2.College of Chemical Engineering,Changchun University of Technology,Changchun,Jilin 130012,China) |
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| Abstract: | For lack of shortcomings of purification of the active ingredient in traditional Chinese medicine,a selective high-prepared supramolecular compound with three-dimensional netlike structure was prepared.The optimum conditions of preparation of resin were ultimately determined by comparing and analyzing the various factors: calcium carbonate as pore-forming agent,20% NaOH concentration,temperature of 50~55 ℃,15% crosslinker,the reaction time of 20 minutes. |
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| Keywords: | resin pore-forming agent β-cyclodextrin |
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