| 低酸度淋洗离子色谱法测定大豆中的植酸 |
| |
| 引用本文： | 黄慧. 低酸度淋洗离子色谱法测定大豆中的植酸[J]. 大连大学学报, 2003, 24(2): 42-44 |
| |
| 作者姓名： | 黄慧 |
| |
| 作者单位： | 大连大学,化学与化学工程系,辽宁,大连,116622 |
| |
| 摘 要： | 本文以含Ca2+、Mg2+的溶液为淋洗液,以Fe(Ⅱ)-磺基水杨酸为柱后衍生体系,在国产分离柱上分离了磷酸与植酸.利用Ca2+、Mg2+与植酸的络合作用缩短了植酸的保留时间,使植酸可在低酸度(pH=4)下被洗脱,实现了植酸的快速离子色谱分析.利用此法,测定大豆样品中植酸的含量,得到满意的结果.
|
| 关 键 词： | 低酸度淋洗 IC法测定 植酸 |
| 文章编号： | 1008-2395(2003)02-0042-03 |
| 修稿时间： | 2002-10-17 |
Determining phytic acid in soybean samples with ion chromatography with an eluent in low acidity |
| |
| HUANG Hui. Determining phytic acid in soybean samples with ion chromatography with an eluent in low acidity[J]. Journal of Dalian University, 2003, 24(2): 42-44 |
| |
| Authors: | HUANG Hui |
| |
| Abstract: | With the solution including Ca2 + , Mg2+ as eluent, with Fe(III)-Ssal as post-column derivation system, phosphonic acid and phytic acid can be separated on a separator column(made in China). Using complexation of the Ca2+, Mg2+ with phytic acid, its retention time can be reduced, the phytic acid can be to eluted by an eluent with low acidity (pH=4) , and its determination with ion chromatography can be done more rapidly. Thus, phytic acid in soybean samples can be determined with this method and satisfactory results can be obtained. |
| |
| Keywords: | elution in low acidity ion chromatography phytic acid |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
