脱铝超稳Y沸石催化合成对羟基苯甲酸异戊酯 |
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引用本文: | 袁先友,周芳启.脱铝超稳Y沸石催化合成对羟基苯甲酸异戊酯[J].零陵学院学报,2002(6). |
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作者姓名: | 袁先友 周芳启 |
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作者单位: | 零陵学院化学系 湖南永州425000
(袁先友),永州市四中 425000(周芳启) |
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摘 要: | 本文研究了脱铝超稳Y沸石催化对羟基苯甲酸与异戊醇的酯化反应,考察了催化剂硅铝比、催化剂用量和反应时间对酯反应的影响.结果表明,在优化反应条件下,反应在6h内完成,酯转化率达58.0%.同时,对水杨酸与异戊醇的酯化反应也进行了研究.
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关 键 词: | 脱铝超稳Y 催化 酯化反应 对羟基苯甲酸异戊酯 |
Catalytic Synthesis of Isoamyl P-Hydroxy-Benzoate by Dealuminated USY |
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Authors: | YUAN Xian-you ZHOU Fang-qi |
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Abstract: | The esterification of p-hydroxy-benzoic acid and isoamyl alcohol by using dealuminated USY as catalyst was studied. The influence of SiO2/Al2O3 ratio in the catalyst, catalyst amount and reaction time were investigated. The experimental results show that under optimum conditions, the esterification could be finished in 6 hour with over 58% yield. At the same time, the esterification of salicylic acid and isoamyl alcohol was also studied. |
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Keywords: | dealuminated USY catalysis esterification isoamyl p-hydroxy-benzoate |
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