| 四氯化锡催化乙酸戊酯的合成研究 |
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| 引用本文： | 杨国臣,薛万华.四氯化锡催化乙酸戊酯的合成研究[J].山西广播电视大学学报,2006,11(3):106-107. |
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| 作者姓名： | 杨国臣 薛万华 |
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| 作者单位： | 雁北师范学院化学系,山西,大同,037009 |
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| 摘 要： | 用四氯化锡取代浓硫酸作为冰乙酸和正戊醇的酯化反应催化剂,成功地合成了乙酸戊酯。在探讨了酯化反应的历程后,找到了较好的反应条件:酸醇摩尔比为1、催化剂用量2.54%、反应时间为60m in,产率达89.9%。
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| 关 键 词： | 乙酸戊酯 四氯化锡 催化 合成 |
| 文章编号： | 1008-8350(2006)03-0106-02 |
| 收稿时间： | 02 28 2006 12:00AM |
| 修稿时间： | 2006年2月28日 |
Study on the Catalytic Synthesis of Banana Oil by Tin Tetrachloride |
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| YANG Guochen,XUE Wanhua.Study on the Catalytic Synthesis of Banana Oil by Tin Tetrachloride[J].Journal of Shanxi Radio & Tv University,2006,11(3):106-107. |
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| Authors: | YANG Guochen XUE Wanhua |
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| Institution: | Department of Chemistry,Yanbei Normal College, Datong, Shanxi, 037009, China |
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| Abstract: | Tin tetrachloride can be used as catalyst for esterification reaction of acetic acid and n-amyl alcohol instead of sulfuric acid.The mechanism of the esterfication reaction and the effect on catalytic reaction were studied. The best conditions were found out: the yield of product can be up to 89.9% for 60 min,the molar ratio of acetic acid and n-amyl alcohol is 1:1.13 and catalyst is 2.54%. |
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| Keywords: | banana oil Tin tetrachloride catalytic synthesis |
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