| N-甲基苯氨基-4,6-二甲氧基-1,3,5三嗪的合成与表征 |
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| 引用本文： | 李宪平,肖深初,熊知行,梅光泉. N-甲基苯氨基-4,6-二甲氧基-1,3,5三嗪的合成与表征[J]. 宜春学院学报, 2006, 28(6): 19-21 |
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| 作者姓名： | 李宪平 肖深初 熊知行 梅光泉 |
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| 作者单位： | 1. 湖南人文科技学院,湖南,娄底,417000
2. 宜春学院,江西,宜春,336000 |
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| 基金项目： | 江西省自然科学基金资助项目(NO.0520083)，江西省教育厅科技计划项目(赣教技字06268)，宜春市社会发展重点科技计划项目(编号:JXYC2005KNA010) |
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| 摘 要： | 目的:为了进一步研究与发展均三嗪衍生物的制备方法.方法:在丙酮介质中,三聚氯氰先后与N-甲基苯胺、甲醇反应,合成了N-甲基苯氨基-4,6-二甲氧基-1,3,5三嗪.结果:标题化合物经红外光谱和质谱对它进行了表征,筛选出了最佳的工艺条件.结论:制备方法简单,反应条件温和,效果良好.
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| 关 键 词： | 三聚氯氰 N-甲基苯氨基-4 6-二甲氧基-1 3 5三嗪 合成 |
| 文章编号： | 1671-380X（2006）06-0019-03 |
| 收稿时间： | 2006-03-29 |
| 修稿时间： | 2006-03-29 |
Synthesis and Characterization of N-methyl-phenylamino-4,6-dimethoxy-1,3,5-triazine |
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| LI Xian-ping,XIAO Shen-chu,XIONG Zhi-xing,MEI Guang-Quan. Synthesis and Characterization of N-methyl-phenylamino-4,6-dimethoxy-1,3,5-triazine[J]. Journal of Yichun University, 2006, 28(6): 19-21 |
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| Authors: | LI Xian-ping XIAO Shen-chu XIONG Zhi-xing MEI Guang-Quan |
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| Affiliation: | 1. Department of Chemistry and Material Science, Hunan Institute of the Humanities, Science and Technology, Loudi 417000 Hunan, China; 2. Yichun University, Yichun 336000 Jiangxi, China |
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| Abstract: | Aim To study and develop synthetic methods of 1,3,5-triazine derivatives further.Method In the medium of acetone,N-methyl-phenylamino-4,6-dimethoxy-1,3,5-triazine has been prepared by the reaction of cyanuric chloride,N-methylaniline and methanol.Results The product has been characterized by IR and MS.Furthermore,the best reaction conditions have been determined.Conclusion This method is simple with mild reaction condition and good effect. |
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| Keywords: | cyanuric chloride N-methyl-phenylamino-4 6-dimethoxy-1 3 5-triazine synthesis |
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