| N,N-二(2,6-二异丙基苯基)-2,4-戊二亚胺和N,N-二(2,6-二甲基苯基)-2,4-戊二亚胺的合成与表征 |
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| 引用本文： | 焦锐,王英.N,N-二(2,6-二异丙基苯基)-2,4-戊二亚胺和N,N-二(2,6-二甲基苯基)-2,4-戊二亚胺的合成与表征[J].连云港师范高等专科学校学报,2007(4):82-83. |
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| 作者姓名： | 焦锐 王英 |
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| 作者单位： | 连云港师范高等专科学校初等教育系,江苏,连云港,222006 |
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| 摘 要： | 以乙酰丙酮、2,6-二异丙基苯胺(或2,6-二甲基苯胺)和对甲苯磺酸为原料通过两步反应高产率的合成了N,N'-二(2,6-二异丙基苯基)-2,4-戊二亚胺(1)和N,N'-二(2,6-二甲基苯基)-2,4-戊二亚胺(2),产率分别为78%和72%,并用元素分析和1HNMR对产物进行了结构表征.
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| 关 键 词： | 乙酰丙酮 2 6-二异丙基苯胺 2 6-二甲基苯胺 对甲苯磺酸 合成 |
| 文章编号： | 1009-7740(2007)04-0082-02 |
| 修稿时间： | 2007年9月28日 |
Synthesis and Characterization of N,N-2,6-diisopropylphenyl-2, 4-pentanediimine and N,N-2,6-dimethylphenyl-2,4-pentanediimine |
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| JIAO Rui,WANG Ying.Synthesis and Characterization of N,N-2,6-diisopropylphenyl-2, 4-pentanediimine and N,N-2,6-dimethylphenyl-2,4-pentanediimine[J].Journal of Lianyungang Teachers College,2007(4):82-83. |
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| Authors: | JIAO Rui WANG Ying |
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| Abstract: | N,N-2,6-diisopropylphenyl-2,4-pentanediimine(1) andN,N-2,6-dimethylphenyl-2,4-pentanediimine(2) were synthesiszed by2,4-pentanedione,2,6-diisopropylamline(or 2,6-dimethylamline) and p-toluene-sulfonie acid.The yields were 78%,72%.The structures of 1 and 2 were confirmed by ER and1HNMR. |
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| Keywords: | 2 4-pentanedione 2 6-diisopropylamline 2 6-dimethylamline p-toluene-sulfonie acid Synthesis |
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