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气相色谱检测白酒中乙酸乙酯内标法和外标法的比较研究
引用本文:徐静,黄建军. 气相色谱检测白酒中乙酸乙酯内标法和外标法的比较研究[J]. 柳州职业技术学院学报, 2006, 6(4): 61-63
作者姓名:徐静  黄建军
作者单位:柳州市产品质量监督检验所,广西,柳州,545001
摘    要:介绍了用气相色谱法测定白酒中己酸乙酯的两种定量方法:内标法和外标法,并分别对三个白酒样品进行测定。测定结果的RSD值依次为0.43%~0.86%和0.46%~1.40%,说明两种定量方法在检测白酒中己酸乙酯时结果无显著性差异,可将外标法推广到日常的白酒检测工作中。

关 键 词:气相色谱法  内标法  外标法  己酸乙酯
文章编号:1671-1084(2006)04-0061-03
收稿时间:2006-05-03
修稿时间:2006-05-23

Comparative Study of Internal Standard Method and External Standard Method of Gas Chromatography Determination of Hexanoic Acetate in Chinese Alcohol
XU Jing,HUANG Jian-jun. Comparative Study of Internal Standard Method and External Standard Method of Gas Chromatography Determination of Hexanoic Acetate in Chinese Alcohol[J]. Journal of Liuzhou Vocational & Technical College, 2006, 6(4): 61-63
Authors:XU Jing  HUANG Jian-jun
Affiliation:Liuzhou Product Quality Supervision Testing Institute, Liuzhou 545001, China
Abstract:This paper introduces the determinating methods of Hexanoic Acetate in Chinese spirits by two quantitative analysis: Internal Standard Method and External Standard Method with Gas Chromatography,by which three samples are determinated.The values of RSD at the range of 0.43% ~ 0.86% are obtained for Internal Standard Method and of 0.46%~1.40% for External Standard Method.It illuminates that there is no remarkable difference in the experiment between two quantitative analysis methods by determinating Hexanoic Acetate in Chinese alcohol,and the External Standard Method can be widely used in determinating the Chinese alcohol.
Keywords:gas chromatography  internal standard method  external standard method  hexanoic acetate
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