| 微波诱导催化糖精N-烷基化反应 |
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| 引用本文： | 钟爱国,杨小平.微波诱导催化糖精N-烷基化反应[J].湘潭师范学院学报(社会科学版),1999(6). |
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| 作者姓名： | 钟爱国 杨小平 |
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| 作者单位： | 台州师专化学系!浙江临海317000(钟爱国)，湘潭师范学院化学系!湖南湘潭411201(杨小平) |
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| 基金项目： | 湖南省重点学科资助项目!湘教通 [1997] 2 0 0号 |
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| 摘 要： | :研究了微波场下用固体碱催化剂干态催化糖精与卤代正庚烷的烷基化反应。探讨了辐射功率、时间、产物提取方式和卤代烷等对产率的影响。结果表明 ,微波场促进了固体碱的催化反应 ,使产率有较大的提高
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| 关 键 词： | 微波辐射 N-烷基化 糖精 |
N-alkylation of saccharin under microwave irradiaton |
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| ZHONG Ai-guo,YANG Xiao-ping.N-alkylation of saccharin under microwave irradiaton[J].Journal of Xiangtan Normal University(Social Science Edition),1999(6). |
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| Authors: | ZHONG Ai-guo YANG Xiao-ping |
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| Abstract: | This paper repots the N-alkylation of Saccharin with alkyl halide under microwave irradiation by using solid reagents as a supporter. The effects of microwave power, irradiation time and the purifying way of product on the alkylation were discussed. |
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| Keywords: | Microwave irradiation n-alkylation saccharin |
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