经血宁颗粒的质量控制标准物质的筛选 |
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引用本文: | 许子竞,唐艳秀,庞国. 经血宁颗粒的质量控制标准物质的筛选[J]. 大众科技, 2014, 0(2): 66-67,79 |
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作者姓名: | 许子竞 唐艳秀 庞国 |
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作者单位: | [1] 广西金秀圣堂药业有限责任公司,广西 金秀545700 [2] 广西大学化学化工学院,广西 南宁530006 |
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摘 要: | 以经血宁颗粒配伍之一的白背叶为原料,经分离纯化得化合物Ⅰ,通过定性鉴定为黄酮苷类;HPLC检测为单一纯化合物;MS测定化其分子量为564;1H NMR和13C NMR数据分析与Corymboside一致,为伞房决明苷,故以化合物Ⅰ作为经血宁颗粒的质量控制标准物质。
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关 键 词: | 白背叶 化合物Ⅰ 伞房决明苷 标准物质 |
Screening standard quality control substance from JingXueNing granules |
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Abstract: | From Mallotus apelta ( Lour.) Muell. -Arg one of JingXueNing granules component,compoundⅠwas getted by the separation and puri-fication and was identified it as flavoniods by qualitative identification. Compounds Ⅰis the single pure compounds by HPLC;the molecular weight of compound Ⅰis 564 by the analysis of MS. The data analysis of 1H NMR and 13C NMR from compoundⅠ is consistent with Corymboside. So the compo-und Ⅰwas as standard quality control substance of JingXueNing granules. |
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Keywords: | Corymboside standard substance |
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