| 红橘果皮中橙皮苷提取工艺研究 |
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| 引用本文： | 王颖,高翔,王卫博,俱卫秀,左彩虹,王灵果,于宏伟.红橘果皮中橙皮苷提取工艺研究[J].石家庄师范专科学校学报,2013(3):32-36,57. |
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| 作者姓名： | 王颖 高翔 王卫博 俱卫秀 左彩虹 王灵果 于宏伟 |
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| 作者单位： | [1]石家庄学院化工学院,河北石家庄050035 [2]河北化工医药职业技术学院化工机械系,河北石家庄050026 |
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| 基金项目： | 河北省科技厅科学技术研究与发展计划（10215687） |
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| 摘 要： | 采用碱浸酸析的方法从红橘果皮中提取橙皮苷．通过对碱的种类、添加量、料液比、提取时间、反应体系pH值及提取温度等因素的研究，确定提取橙皮苷的最佳工艺条件为：温度在30℃，在25g的橘皮粉中加入750g蒸馏水，1．75g氢氧化钙，搅拌浸提0．5h，酸析的pH值为3，粗产品收率为4．2％．粗产品经过重结晶分离提纯，收率达到56％，产品结构经过IR鉴定．
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| 关 键 词： | 橙皮苷 碱浸酸析 提取工艺 研究 红外 |
Study on Extraction Technology of Hesperidine from Mandarin Peel |
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| WANG Ying,GAO Xiang,WANG Wei-bo,JU Wei-xiu,ZUO Cai-hong,WANG Ling.guo,YU Hong-wei.Study on Extraction Technology of Hesperidine from Mandarin Peel[J].Journal of Shijiazhuang Teachers College,2013(3):32-36,57. |
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| Authors: | WANG Ying GAO Xiang WANG Wei-bo JU Wei-xiu ZUO Cai-hong WANG Lingguo YU Hong-wei |
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| Institution: | 1.School of Chemical Engineering,Shijiazhuang University,Shijiazhuang,Hebei 050035,China; 2. Hebei Vocational College of Chemical ＆ Pharmaceutical Technology Department of Chemical Engineering Mechanics, Shijiazhuang, Hebei 050026, China) |
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| Abstract: | Hesperidin was extracted from mandarin peel by alkali leaching acid precipitation method. The Optimum process conditions were studied with base, additive amount,feed liquid ratio,time,pH and temperature. The best process condition was 30 ℃, 25 g mandarin peel, 750 g distilled water, 1.75 g calcium hydroxide, 0.5 h, pH=3. The crude product yield was 4.2%. The crude was purified by recrystallization, and the yield was 56%. The product was characterized by IR. |
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| Keywords: | Hesperidine Alkali leaching acid precipitation extraction process research IR |
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